Abstract:In order to recycle the valuable minerals ,such as tantalum niobite ,columbite-tantalite and mi-crolite ,beneficiation test is carried out for the tantalum-niobium ore , the ore deposit of w hich is large granite .The tantalum niobium concentrate with 6 .89, grade and 57 .482, recovery is achieved after the mineral has been treated by two-stage grinding and two-stage separation ,rough concentrate is obtained by single gravity separation during the roughing , the scheme gravity-flotation-gravity is used in cleaning . Tantalum niobium slag with 29 .0, Ta2 O5 and 53 .487, recovery for raw ore is received after the impuri-ties such as tungsten ,tin ,silicon are removed by hydrometallurgy .